Quantification of hindered phenols in polyamide 11 during thermal aging
dc.contributor.author | OKAMBA-DIOGO, Octavie |
dc.contributor.author | VERDU, Jacques |
dc.contributor.author
hal.structure.identifier | FERNAGUT, François
|
dc.contributor.author
hal.structure.identifier | GUILMENT, Jean
|
dc.contributor.author
hal.structure.identifier | PERY, Frédérique
|
dc.contributor.author
hal.structure.identifier | FAYOLLE, Bruno
|
dc.contributor.author | RICHAUD, Emmanuel |
dc.date.accessioned | 2016 |
dc.date.available | 2017 |
dc.date.issued | 2016 |
dc.date.submitted | 2016 |
dc.identifier.issn | 0142-9418 |
dc.identifier.uri | http://hdl.handle.net/10985/10714 |
dc.description.abstract | Polyamide 11 films stabilized by Irganox® 1098, Irganox® 1010 or Irganox® 245 were subjected to thermal oxidation at 110°C. The residual phenol content was assessed by comparing three analytical methods:high performance liquid chromatography (HPLC), determination of the Oxidation Induction Time (OIT)and Onset Oxidation Temperature (OOT) by thermal analyses. Both OIT and OOT are reliable for virgin PA11 after a relevant calibration by HPLC measurement. In the case of oxidized samples, OOT measurements have the benefits of being more easily interpretable than OIT and less time-consuming than HPLC measurements. |
dc.description.sponsorship | CIFRE |
dc.language.iso | en |
dc.publisher | Elsevier |
dc.rights | Post-print |
dc.subject | Polyamide |
dc.subject | Hindered phenol |
dc.subject | Thermal analysis |
dc.subject | HPLC |
dc.subject | Thermal oxidation |
dc.title | Quantification of hindered phenols in polyamide 11 during thermal aging |
ensam.embargo.terms | 2018-03-30 |
dc.identifier.doi | 10.1016/j.polymertesting.2016.03.023 |
dc.typdoc | Article dans une revue avec comité de lecture |
dc.localisation | Centre de Paris |
dc.subject.hal | Chimie: Matériaux |
dc.subject.hal | Chimie: Polymères |
dc.subject.hal | Sciences de l'ingénieur: Matériaux |
ensam.audience | Internationale |
ensam.page | 63-70 |
ensam.journal | Polymer Testing |
ensam.volume | 52 |
ensam.peerReviewing | Oui |
hal.identifier | hal-01304276 |
hal.version | 1 |
hal.status | accept |