In situ observation of g-ZrH formation by X-ray diffraction
dc.contributor.author | MAIMAITIYILIT, Tuerdi |
dc.contributor.author | BJERKEN, Christina |
dc.contributor.author
hal.structure.identifier | STEUWER, Axel
|
dc.contributor.author | WANG, Z |
dc.contributor.author | DANIELS, J |
dc.contributor.author
hal.structure.identifier | ANDRIEUX, Jérôme
|
dc.contributor.author | BLOMQVIST, Jakob |
dc.contributor.author
hal.structure.identifier | ZANELLATO, Olivier
|
dc.date.accessioned | 2018 |
dc.date.available | 2018 |
dc.date.issued | 2017 |
dc.date.submitted | 2017 |
dc.identifier.issn | 0925-8388 |
dc.identifier.uri | http://hdl.handle.net/10985/12465 |
dc.description.abstract | We report on the measurement of the formation of γ-ZrH during in situ gaseous charging. The measurements were undertaken using high-energy synchrotron X-ray diffraction. Experimental observation shows that γ-ZrH can form at 180 °C from a mixture of α+δ while dehydrogenating at slow cooling rates. The observation is further supported by ex situ laboratory X-ray diffraction on deuterated Zr powder that has undergone a similar heat-treatment cycle. The crystal structure of γ-ZrH refinement agrees with the reported P42/n structure found in the literature. |
dc.language.iso | en |
dc.publisher | Elsevier |
dc.rights | Post-print |
dc.subject | Zirconium hydride |
dc.subject | g-ZrH |
dc.subject | Synchrotron X-ray diffraction |
dc.subject | Hydrogen charging |
dc.title | In situ observation of g-ZrH formation by X-ray diffraction |
dc.identifier.doi | 10.1016/j.jallcom.2016.11.337 |
dc.typdoc | Article dans une revue avec comité de lecture |
dc.localisation | Centre de Paris |
dc.subject.hal | Sciences de l'ingénieur: Matériaux |
dc.subject.hal | Sciences de l'ingénieur: Mécanique |
ensam.audience | Internationale |
ensam.page | 3124-3130 |
ensam.journal | Journal of Alloys and Compounds |
ensam.volume | 695 |
ensam.peerReviewing | Oui |
hal.status | unsent |