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<title>SAM</title>
<link>https://sam.ensam.eu:443</link>
<description>The DSpace digital repository system captures, stores, indexes, preserves, and distributes digital research material.</description>
<pubDate xmlns="http://apache.org/cocoon/i18n/2.1">Sun, 07 Jun 2026 14:33:46 GMT</pubDate>
<dc:date>2026-06-07T14:33:46Z</dc:date>
<item>
<title>Low friction MoS2TiW Coatings Manufactured on X38CrMoV5-1 Steel Using PVD Method</title>
<link>http://hdl.handle.net/10985/8110</link>
<description>Low friction MoS2TiW Coatings Manufactured on X38CrMoV5-1 Steel Using PVD Method
GOŁĄBCZAK, Marcin; JACQUET, Philippe; NOUVEAU, Corinne; FLITI, Romain
In this  article the  friction  coefficients and  the  wear  resistances of MoS2TiW protective coatings manufactured on X38CrMoV5-1 steel  samples by using PVD technology are studied. The investi- gations based  on tribometer tests which  were  carried out  in different temperature conditions. The process of deposition of PVD coatings was  realized by using  multisource, hybrid  factory- scale equipment of type URM 079. This equipment allows for deposition of coatings by the phys- ical method. The tribological tests were  performed using a precision high temperature tribome- ter  under ambient and  high temperature conditions with  a steel  and  corundum balls as coun- ter-samples. In this  paper the  results of these tribological tests are  presented. It is shown  that the  measured friction  coefficient of steel  samples with  PVD coatings is significantly lower  than the  friction  coefficient of uncoated steel.  It is also shown  that X38CrMoV5-1 steel  samples with manufactured MoS2TiW coatings are  characterized by very  low  friction  coefficient and  high wear  resistance.
</description>
<pubDate>Tue, 01 Jan 2013 00:00:00 GMT</pubDate>
<guid isPermaLink="false">http://hdl.handle.net/10985/8110</guid>
<dc:date>2013-01-01T00:00:00Z</dc:date>
<dc:creator>GOŁĄBCZAK, Marcin</dc:creator>
<dc:creator>JACQUET, Philippe</dc:creator>
<dc:creator>NOUVEAU, Corinne</dc:creator>
<dc:creator>FLITI, Romain</dc:creator>
<dc:description>In this  article the  friction  coefficients and  the  wear  resistances of MoS2TiW protective coatings manufactured on X38CrMoV5-1 steel  samples by using PVD technology are studied. The investi- gations based  on tribometer tests which  were  carried out  in different temperature conditions. The process of deposition of PVD coatings was  realized by using  multisource, hybrid  factory- scale equipment of type URM 079. This equipment allows for deposition of coatings by the phys- ical method. The tribological tests were  performed using a precision high temperature tribome- ter  under ambient and  high temperature conditions with  a steel  and  corundum balls as coun- ter-samples. In this  paper the  results of these tribological tests are  presented. It is shown  that the  measured friction  coefficient of steel  samples with  PVD coatings is significantly lower  than the  friction  coefficient of uncoated steel.  It is also shown  that X38CrMoV5-1 steel  samples with manufactured MoS2TiW coatings are  characterized by very  low  friction  coefficient and  high wear  resistance.</dc:description>
</item>
<item>
<title>Nano- and micro-scale morghological defects in oxidized a-SiC: H thin films</title>
<link>http://hdl.handle.net/10985/10088</link>
<description>Nano- and micro-scale morghological defects in oxidized a-SiC: H thin films
VASIN, Andriy; GOMENIUK, Yuri; RUSAVSKY, Audrey; NAZAROV, Alexey N.; LYSENKO, V.S.; LYTVYN, Petro M.; GONTAR, O.G.; STARIK, Sergii P.; ASHOK, S.; NOUVEAU, Corinne
Amorphous carbon rich a-SiC:H films were deposited on silicon substrates by RF-magnetron sputtering of SiC target in argon/methane gas mixture. The principal focus of this study was investigation of the effect of thermal oxidation on structure and morphology reconstruction in a-SiC:H amorphous network. The density of the films was varied over the range 1.6-2.2 g/cm2 by varying the magnetron discharge power. The local nano- and micro-scale surface morphology and chemical composition distribution were examined by atomic force microscopy, scanning electron microscopy equipped with Auger electron scanning system and optical profilometry. It was found that partial oxidation leads to local structure reconstruction accompanied by transformation of mechanical stresses from compressive to tensile. Formation of carbon-enriched nano- and micro-scale regions was observed after oxidation in low density samples. We attrribute these morphological defects to migration and precipitation of carbon species released in the process of oxidation of the SiC amorphous network. The mechanism of tensile stresses generation is also discussed.
</description>
<pubDate>Tue, 01 Jan 2013 00:00:00 GMT</pubDate>
<guid isPermaLink="false">http://hdl.handle.net/10985/10088</guid>
<dc:date>2013-01-01T00:00:00Z</dc:date>
<dc:creator>VASIN, Andriy</dc:creator>
<dc:creator>GOMENIUK, Yuri</dc:creator>
<dc:creator>RUSAVSKY, Audrey</dc:creator>
<dc:creator>NAZAROV, Alexey N.</dc:creator>
<dc:creator>LYSENKO, V.S.</dc:creator>
<dc:creator>LYTVYN, Petro M.</dc:creator>
<dc:creator>GONTAR, O.G.</dc:creator>
<dc:creator>STARIK, Sergii P.</dc:creator>
<dc:creator>ASHOK, S.</dc:creator>
<dc:creator>NOUVEAU, Corinne</dc:creator>
<dc:description>Amorphous carbon rich a-SiC:H films were deposited on silicon substrates by RF-magnetron sputtering of SiC target in argon/methane gas mixture. The principal focus of this study was investigation of the effect of thermal oxidation on structure and morphology reconstruction in a-SiC:H amorphous network. The density of the films was varied over the range 1.6-2.2 g/cm2 by varying the magnetron discharge power. The local nano- and micro-scale surface morphology and chemical composition distribution were examined by atomic force microscopy, scanning electron microscopy equipped with Auger electron scanning system and optical profilometry. It was found that partial oxidation leads to local structure reconstruction accompanied by transformation of mechanical stresses from compressive to tensile. Formation of carbon-enriched nano- and micro-scale regions was observed after oxidation in low density samples. We attrribute these morphological defects to migration and precipitation of carbon species released in the process of oxidation of the SiC amorphous network. The mechanism of tensile stresses generation is also discussed.</dc:description>
</item>
<item>
<title>Effect of the sand-blasting of edge peeling tools on the cutting forces and wear resistance</title>
<link>http://hdl.handle.net/10985/8315</link>
<description>Effect of the sand-blasting of edge peeling tools on the cutting forces and wear resistance
LABIDI, Chafik; HENRY, Laurent; NOUVEAU, Corinne; DENAUD, Louis; COLLET, Robert
One of the major problems concerning tools of wood industry is nicks occurrence on the cutting edge. This phenomenon is accentuated by the small tool angle of most of the wood machining tools. The aim of this present study is to look if the geometry modifications of the cutting edge permit to decrease the weakness of the tools, especially in peeling process. For this, different sand-blasted tools were tested in laboratory peeling of beech. In addition, the adhesion of CrAlN hard coating deposited on a modified cutting edge was also explored. The results obtained showed that the artificial wear by sand-blasting permits to increase the shocks resistance, coatings anchoring and changes the wear mechanism of the tools.
</description>
<pubDate>Mon, 01 Jan 2007 00:00:00 GMT</pubDate>
<guid isPermaLink="false">http://hdl.handle.net/10985/8315</guid>
<dc:date>2007-01-01T00:00:00Z</dc:date>
<dc:creator>LABIDI, Chafik</dc:creator>
<dc:creator>HENRY, Laurent</dc:creator>
<dc:creator>NOUVEAU, Corinne</dc:creator>
<dc:creator>DENAUD, Louis</dc:creator>
<dc:creator>COLLET, Robert</dc:creator>
<dc:description>One of the major problems concerning tools of wood industry is nicks occurrence on the cutting edge. This phenomenon is accentuated by the small tool angle of most of the wood machining tools. The aim of this present study is to look if the geometry modifications of the cutting edge permit to decrease the weakness of the tools, especially in peeling process. For this, different sand-blasted tools were tested in laboratory peeling of beech. In addition, the adhesion of CrAlN hard coating deposited on a modified cutting edge was also explored. The results obtained showed that the artificial wear by sand-blasting permits to increase the shocks resistance, coatings anchoring and changes the wear mechanism of the tools.</dc:description>
</item>
<item>
<title>Influence de l’orientation du fil sur les efforts de coupe dans le défonçage du Pin d’Alep</title>
<link>http://hdl.handle.net/10985/7536</link>
<description>Influence de l’orientation du fil sur les efforts de coupe dans le défonçage du Pin d’Alep
AKNOUCHE, Hamid; ZERIZER, Abdellatif; MARCHAL, Rémy; BUTAUD, Jean-Claude; NOUVEAU, Corinne
Ce travail a pour but final de mesurer les forces de coupe dans le domaine du défonçage du Pin d’Alep en fonction de différents angles du fil. La mesure des forces de coupe a été faite grâce a une table piézo-électrique a trois axes, montée sur la table d’une défonceuse a commande numérique. L’outil de coupe représente une fraise sur laquelle est monté une plaquette en carbure faisant un mouvement de rotation et circulaire, ce qui nous donne une variation de l’angle du grain d’une manière instantané.
</description>
<pubDate>Sun, 01 Jan 2006 00:00:00 GMT</pubDate>
<guid isPermaLink="false">http://hdl.handle.net/10985/7536</guid>
<dc:date>2006-01-01T00:00:00Z</dc:date>
<dc:creator>AKNOUCHE, Hamid</dc:creator>
<dc:creator>ZERIZER, Abdellatif</dc:creator>
<dc:creator>MARCHAL, Rémy</dc:creator>
<dc:creator>BUTAUD, Jean-Claude</dc:creator>
<dc:creator>NOUVEAU, Corinne</dc:creator>
<dc:description>Ce travail a pour but final de mesurer les forces de coupe dans le domaine du défonçage du Pin d’Alep en fonction de différents angles du fil. La mesure des forces de coupe a été faite grâce a une table piézo-électrique a trois axes, montée sur la table d’une défonceuse a commande numérique. L’outil de coupe représente une fraise sur laquelle est monté une plaquette en carbure faisant un mouvement de rotation et circulaire, ce qui nous donne une variation de l’angle du grain d’une manière instantané.</dc:description>
</item>
<item>
<title>Test d’usure d’outils modifiés ou non lors du déroulage de MDF</title>
<link>http://hdl.handle.net/10985/7492</link>
<description>Test d’usure d’outils modifiés ou non lors du déroulage de MDF
AKNOUCHE, Hamid; BENLATRECHE, Yacine; ROUSSELOT, Christophe; PILLOUD, David; ZERIZER, Abdellatif; MARCHAL, Rémy; NOUVEAU, Corinne
Des revêtements à base de nitrure de chrome réalisés par pulvérisation triode ont été testés en déroulage et défonçage du bois. L’efficacité des revêtements triode a été montrée en usinage de MDF (Medium Density Fiberboard), donc dans des conditions sévères de coupe, ainsi qu’en défonçage d’OSB (Oriented Strand Board) où un revêtement CrN de 1μm d’épaisseur permet d’usiner 9 fois plus qu’un outil non revêtu [1]. Le but de cette étude est d’examiner comment on peut améliorer la tenue à l’usure des outils de coupe dans l’opération de déroulage du MDF, en traitant la partie active de l’outil. Les modifications des surfaces actives des couteaux consistent à appliquer des films durs (CrAlN, CrSiN), qui ont déjà donné des résultats prometteurs dans l’opération de défonçage du MDF [2], l’un des facteurs limitant dont il faut nous affranchir est l’adhérence des couches déposées sur les outils de coupe. C’est pourquoi nous avons testé des traitements duplex (nitruration ionique+dépôt magnétron). Ces revêtements ont également été testés en simulant les chocs que peuvent générer les noeuds dans un billon. Les revêtements de CrAlN ont été réalisés par PVD sur un bâti dual magnétron RF alors que les couches de CrSiN ont été obtenues par l’institut FEMTO/ST de Besançon dans le cadre d’un projet de recherche. La nitruration ionique a été réalisée dans un four de traitement thermochimique BMI. Le processus d’usinage a été effectué sur une microdérouleuse instrumentée, le matériau utilisé étant du MDF (Medium Density Fiberboard).
</description>
<pubDate>Fri, 01 Jan 2010 00:00:00 GMT</pubDate>
<guid isPermaLink="false">http://hdl.handle.net/10985/7492</guid>
<dc:date>2010-01-01T00:00:00Z</dc:date>
<dc:creator>AKNOUCHE, Hamid</dc:creator>
<dc:creator>BENLATRECHE, Yacine</dc:creator>
<dc:creator>ROUSSELOT, Christophe</dc:creator>
<dc:creator>PILLOUD, David</dc:creator>
<dc:creator>ZERIZER, Abdellatif</dc:creator>
<dc:creator>MARCHAL, Rémy</dc:creator>
<dc:creator>NOUVEAU, Corinne</dc:creator>
<dc:description>Des revêtements à base de nitrure de chrome réalisés par pulvérisation triode ont été testés en déroulage et défonçage du bois. L’efficacité des revêtements triode a été montrée en usinage de MDF (Medium Density Fiberboard), donc dans des conditions sévères de coupe, ainsi qu’en défonçage d’OSB (Oriented Strand Board) où un revêtement CrN de 1μm d’épaisseur permet d’usiner 9 fois plus qu’un outil non revêtu [1]. Le but de cette étude est d’examiner comment on peut améliorer la tenue à l’usure des outils de coupe dans l’opération de déroulage du MDF, en traitant la partie active de l’outil. Les modifications des surfaces actives des couteaux consistent à appliquer des films durs (CrAlN, CrSiN), qui ont déjà donné des résultats prometteurs dans l’opération de défonçage du MDF [2], l’un des facteurs limitant dont il faut nous affranchir est l’adhérence des couches déposées sur les outils de coupe. C’est pourquoi nous avons testé des traitements duplex (nitruration ionique+dépôt magnétron). Ces revêtements ont également été testés en simulant les chocs que peuvent générer les noeuds dans un billon. Les revêtements de CrAlN ont été réalisés par PVD sur un bâti dual magnétron RF alors que les couches de CrSiN ont été obtenues par l’institut FEMTO/ST de Besançon dans le cadre d’un projet de recherche. La nitruration ionique a été réalisée dans un four de traitement thermochimique BMI. Le processus d’usinage a été effectué sur une microdérouleuse instrumentée, le matériau utilisé étant du MDF (Medium Density Fiberboard).</dc:description>
</item>
<item>
<title>Couches minces dures type Cr-Al-N pour outils de coupe du bois</title>
<link>http://hdl.handle.net/10985/7546</link>
<description>Couches minces dures type Cr-Al-N pour outils de coupe du bois
AKNOUCHE, Hamid; ZERIZER, Abdellatif; KENNOUCHE, Salim; SITOUAH, N.; BOULAHIA, H.; NOUVEAU, Corinne
Les outils de coupe pour l’usinage métallique sont très développés ces dernières années, ainsi plus 90% des outils en carbure et 10% des forets, tarauds en acier sont revêtus, tout en donnant des résultats intéressants, malheureusement cette tendance n’existe pas en usinage bois. Ce travail donc a pour objectif de développer des outils revêtus pour les tester en défonçage du bois de Pin d’Alep une essence très répandues dans le bassin méditerranéen. Notre étude se fera sur des outils de coupe en carbure revêtu en couches minces de CrN et de CrAlN  à différent pourcentage respectivement d’Al déposé  grâce à un bâti magnétron de marque Nordiko 3500.Les conditions de dépôts sont optimisés lors des précédents travaux, les essais d’usinage sont réalisés sur une défonceuse à commande numérique de marque Recordi. Le comportement à l’usure des outils modifiés est avéré très prometteur, on a constaté que les films en nitrure de chrome résistent d’une manière considérable par rapport aux outils en carbures. L’ajout de l’Aluminium n’améliore pas la résistance à l’usure mais contribue à la cristallisation des films.
</description>
<pubDate>Tue, 01 Jan 2013 00:00:00 GMT</pubDate>
<guid isPermaLink="false">http://hdl.handle.net/10985/7546</guid>
<dc:date>2013-01-01T00:00:00Z</dc:date>
<dc:creator>AKNOUCHE, Hamid</dc:creator>
<dc:creator>ZERIZER, Abdellatif</dc:creator>
<dc:creator>KENNOUCHE, Salim</dc:creator>
<dc:creator>SITOUAH, N.</dc:creator>
<dc:creator>BOULAHIA, H.</dc:creator>
<dc:creator>NOUVEAU, Corinne</dc:creator>
<dc:description>Les outils de coupe pour l’usinage métallique sont très développés ces dernières années, ainsi plus 90% des outils en carbure et 10% des forets, tarauds en acier sont revêtus, tout en donnant des résultats intéressants, malheureusement cette tendance n’existe pas en usinage bois. Ce travail donc a pour objectif de développer des outils revêtus pour les tester en défonçage du bois de Pin d’Alep une essence très répandues dans le bassin méditerranéen. Notre étude se fera sur des outils de coupe en carbure revêtu en couches minces de CrN et de CrAlN  à différent pourcentage respectivement d’Al déposé  grâce à un bâti magnétron de marque Nordiko 3500.Les conditions de dépôts sont optimisés lors des précédents travaux, les essais d’usinage sont réalisés sur une défonceuse à commande numérique de marque Recordi. Le comportement à l’usure des outils modifiés est avéré très prometteur, on a constaté que les films en nitrure de chrome résistent d’une manière considérable par rapport aux outils en carbures. L’ajout de l’Aluminium n’améliore pas la résistance à l’usure mais contribue à la cristallisation des films.</dc:description>
</item>
<item>
<title>Effect of layer thickness on thermal properties of multilayer thin films produced by PVD</title>
<link>http://hdl.handle.net/10985/8356</link>
<description>Effect of layer thickness on thermal properties of multilayer thin films produced by PVD
TLILI, Brahim; WALOCK, Michael J.; NASRI, Mustapha; GHRIB, Taher; NOUVEAU, Corinne
Cr/CrN/CrAlN, CrN/CrAlN and Cr/CrN thin layers were deposited by PVD (Physical Vapor Deposition). The multilayers were obtained from the combined deposition of different layers Cr, CrN and CrAlN thick films on on AISI4140 steel and silicon substrates at 200 °C, and evaluated with respect to fundamental properties such as structure and thermal properties. Cr, CrN and CrAlN single layers were also prepared for comparison purposes. The structural and morphological properties of PVD layers were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM) coupled with EDS + WDS microanalyses, stresses were determined by the Newton’s rings methods using the Stoney’s equation and surface hardening and hardness profiles were evaluated by micro hardness measurements. The XRD data and HRTEM showed that both the Cr/CrN, CrN/CrAlN and Cr/CrN/CrAlN multilayer coatings exhibited B1NaCl structure with a prominent reflection along (200) plane, and CrAlN sub-layer microstructures composed of nanocrystallites uniformly embedded in an amorphous matrix. The innovation of this work was to use the thickness of three different coating types to determine the thermal properties. Furthermore, an empirical equation was developed for the thermal properties variations with temperature of AISI4140 steel coated with different multilayer coatings. The thermal conductivity of CrAlN single layered was lower than the multilayer and the bulk material AISI4140. Moreover, the influences of structure and composition of the multilayer coatings on the thermal properties are discussed.  The thermal conductivity of nanoscale thin film is remarkably lower than that of bulk materials because of its various size effects.
</description>
<pubDate>Sun, 01 Jan 2012 00:00:00 GMT</pubDate>
<guid isPermaLink="false">http://hdl.handle.net/10985/8356</guid>
<dc:date>2012-01-01T00:00:00Z</dc:date>
<dc:creator>TLILI, Brahim</dc:creator>
<dc:creator>WALOCK, Michael J.</dc:creator>
<dc:creator>NASRI, Mustapha</dc:creator>
<dc:creator>GHRIB, Taher</dc:creator>
<dc:creator>NOUVEAU, Corinne</dc:creator>
<dc:description>Cr/CrN/CrAlN, CrN/CrAlN and Cr/CrN thin layers were deposited by PVD (Physical Vapor Deposition). The multilayers were obtained from the combined deposition of different layers Cr, CrN and CrAlN thick films on on AISI4140 steel and silicon substrates at 200 °C, and evaluated with respect to fundamental properties such as structure and thermal properties. Cr, CrN and CrAlN single layers were also prepared for comparison purposes. The structural and morphological properties of PVD layers were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM) coupled with EDS + WDS microanalyses, stresses were determined by the Newton’s rings methods using the Stoney’s equation and surface hardening and hardness profiles were evaluated by micro hardness measurements. The XRD data and HRTEM showed that both the Cr/CrN, CrN/CrAlN and Cr/CrN/CrAlN multilayer coatings exhibited B1NaCl structure with a prominent reflection along (200) plane, and CrAlN sub-layer microstructures composed of nanocrystallites uniformly embedded in an amorphous matrix. The innovation of this work was to use the thickness of three different coating types to determine the thermal properties. Furthermore, an empirical equation was developed for the thermal properties variations with temperature of AISI4140 steel coated with different multilayer coatings. The thermal conductivity of CrAlN single layered was lower than the multilayer and the bulk material AISI4140. Moreover, the influences of structure and composition of the multilayer coatings on the thermal properties are discussed.  The thermal conductivity of nanoscale thin film is remarkably lower than that of bulk materials because of its various size effects.</dc:description>
</item>
<item>
<title>Etude des propriétés microstructurales, mécaniques, thermiques et de la porosité des couches minces de CrAlN déposées par PVD sous différents pourcentages d’aluminium</title>
<link>http://hdl.handle.net/10985/7545</link>
<description>Etude des propriétés microstructurales, mécaniques, thermiques et de la porosité des couches minces de CrAlN déposées par PVD sous différents pourcentages d’aluminium
TLILI, Brahim; BENLATRECHE, Yacine; GHRIB, Taher; NOUVEAU, Corinne
Several experimental investigations have led to the development of CrAlN (Chrome Aluminum Nitride) hard coatings by varying the aluminum target bias voltage, in preference to the traditional CrN coating. The present work enabled characterisation by physical and mechanical techniques (XRD, AFM, MEB, nano-indentation, Young’s modulus, thermal propriety, Stress, porosity, etc.). Moreover, in order to find improved the adhesion of the different deposition condition of the coatings. The results obtained in this work demonstrate that variation in proportion to aluminum alter the resulting columnar morphology and porosity of the coatings. The thermal properties and the physical property are greatly affected by these morphological alterations. The comparison between the different coating microstructures of CrAlN coatings (columnar and fine-grained) reveals advantages for the fine-grained structure. The results are better wear protection and less profile deviation. Correlation between aluminum proportions in CrAlN coatings and his thermal properties revealed that the conductivity and the diffusivity are influenced primarily by size and shape distribution of the pores and secondarily by decrease of the stitch parameter dimension.
</description>
<pubDate>Tue, 01 Jan 2008 00:00:00 GMT</pubDate>
<guid isPermaLink="false">http://hdl.handle.net/10985/7545</guid>
<dc:date>2008-01-01T00:00:00Z</dc:date>
<dc:creator>TLILI, Brahim</dc:creator>
<dc:creator>BENLATRECHE, Yacine</dc:creator>
<dc:creator>GHRIB, Taher</dc:creator>
<dc:creator>NOUVEAU, Corinne</dc:creator>
<dc:description>Several experimental investigations have led to the development of CrAlN (Chrome Aluminum Nitride) hard coatings by varying the aluminum target bias voltage, in preference to the traditional CrN coating. The present work enabled characterisation by physical and mechanical techniques (XRD, AFM, MEB, nano-indentation, Young’s modulus, thermal propriety, Stress, porosity, etc.). Moreover, in order to find improved the adhesion of the different deposition condition of the coatings. The results obtained in this work demonstrate that variation in proportion to aluminum alter the resulting columnar morphology and porosity of the coatings. The thermal properties and the physical property are greatly affected by these morphological alterations. The comparison between the different coating microstructures of CrAlN coatings (columnar and fine-grained) reveals advantages for the fine-grained structure. The results are better wear protection and less profile deviation. Correlation between aluminum proportions in CrAlN coatings and his thermal properties revealed that the conductivity and the diffusivity are influenced primarily by size and shape distribution of the pores and secondarily by decrease of the stitch parameter dimension.</dc:description>
</item>
<item>
<title>Structural, microstructural, and optical properties of Zn1−xMg xO thin films grown onto glass substrate by ultrasonic spray pyrolysis</title>
<link>http://hdl.handle.net/10985/10096</link>
<description>Structural, microstructural, and optical properties of Zn1−xMg xO thin films grown onto glass substrate by ultrasonic spray pyrolysis
HOGGAS, Khadra; DJELLOUL, Abdelkader; BOUOUDINA, M.; NOUVEAU, Corinne
Pure and doped Zn1−xMgxO films were deposited onto glass substrate by ultrasonic spray pyrolysis technique. The variation of lattice constant and the blue shift of near-band-edge emission indicate that Zn2+ ions are successfully substituted by Mg2+ ions within ZnO lattice. At higher Mg content (x ≥ 0.21), a drastic change appears in the morphology, as a result of structural changes from wurtzite (ZnO) structure into a mixture of wurtzite and cubic (MgO) phases. FTIR study indicated the existence of distinct characteristic absorption peaks at ~442 cm−1 for Zn–O stretching mode that shifted toward the red region with the increase in Mg content. In addition to the host phonons of ZnO, one additional band was observed around 523 cm−1, presumably attributed to the Mg-related vibrational mode. The optical constants and thickness of thin films have been determined using experimental transmittance data. The luminescence intensity at 2.63 eV of Zn0.85Mg0.15O thin films was found to be approximately 13 times higher than that of pure ZnO film measured under the same excitation conditions
</description>
<pubDate>Thu, 01 Jan 2015 00:00:00 GMT</pubDate>
<guid isPermaLink="false">http://hdl.handle.net/10985/10096</guid>
<dc:date>2015-01-01T00:00:00Z</dc:date>
<dc:creator>HOGGAS, Khadra</dc:creator>
<dc:creator>DJELLOUL, Abdelkader</dc:creator>
<dc:creator>BOUOUDINA, M.</dc:creator>
<dc:creator>NOUVEAU, Corinne</dc:creator>
<dc:description>Pure and doped Zn1−xMgxO films were deposited onto glass substrate by ultrasonic spray pyrolysis technique. The variation of lattice constant and the blue shift of near-band-edge emission indicate that Zn2+ ions are successfully substituted by Mg2+ ions within ZnO lattice. At higher Mg content (x ≥ 0.21), a drastic change appears in the morphology, as a result of structural changes from wurtzite (ZnO) structure into a mixture of wurtzite and cubic (MgO) phases. FTIR study indicated the existence of distinct characteristic absorption peaks at ~442 cm−1 for Zn–O stretching mode that shifted toward the red region with the increase in Mg content. In addition to the host phonons of ZnO, one additional band was observed around 523 cm−1, presumably attributed to the Mg-related vibrational mode. The optical constants and thickness of thin films have been determined using experimental transmittance data. The luminescence intensity at 2.63 eV of Zn0.85Mg0.15O thin films was found to be approximately 13 times higher than that of pure ZnO film measured under the same excitation conditions</dc:description>
</item>
<item>
<title>A study of the tribological behavior of duplex treatment</title>
<link>http://hdl.handle.net/10985/10878</link>
<description>A study of the tribological behavior of duplex treatment
SIAD, Ahcene; NOUVEAU, Corinne; BESNARD, Aurélien; JACQUET, Philippe; QUESADA, Jean
The objective of this study is to determine the influence of duplex treatment (low pressure thermochemical treatment and PVD coating) on tribological properties. The carbide and carbonitride coatings are deposited by dual RF magnetron sputtering on the reference steel 18CrMo4 and the carburized and carbonitrided one (respectively). The low-pressure carburized and carbonitrided samples present 0.72 and 0.69 w. % carbon content at their surface respectively and a hardness of about 700 Hv0.1. The carburizing and carbonitriding layer are respectively 540 and 390 µm thick, while TiWC and TiWCN were 2.8 and 3.4 µm thick respectively. Tribological tests were performed by a Pin-on-Disk rotative tribometer with alumina and steel (100Cr6) balls. A comparison of the friction coefficient and the wear rate for each sample has been made. The adhesion of the coatings has been performed by analyzing the wear track using optical profilometry, optical microscopy and scanning electron microscopy equipped with an energy-dispersive X-ray spectrometer. The best tribological performances were observed by combining carbides coatings and carburized 18CrMo4 or reference steel. In contrast, the TiWCN thin film completely delaminated.
</description>
<pubDate>Thu, 01 Jan 2015 00:00:00 GMT</pubDate>
<guid isPermaLink="false">http://hdl.handle.net/10985/10878</guid>
<dc:date>2015-01-01T00:00:00Z</dc:date>
<dc:creator>SIAD, Ahcene</dc:creator>
<dc:creator>NOUVEAU, Corinne</dc:creator>
<dc:creator>BESNARD, Aurélien</dc:creator>
<dc:creator>JACQUET, Philippe</dc:creator>
<dc:creator>QUESADA, Jean</dc:creator>
<dc:description>The objective of this study is to determine the influence of duplex treatment (low pressure thermochemical treatment and PVD coating) on tribological properties. The carbide and carbonitride coatings are deposited by dual RF magnetron sputtering on the reference steel 18CrMo4 and the carburized and carbonitrided one (respectively). The low-pressure carburized and carbonitrided samples present 0.72 and 0.69 w. % carbon content at their surface respectively and a hardness of about 700 Hv0.1. The carburizing and carbonitriding layer are respectively 540 and 390 µm thick, while TiWC and TiWCN were 2.8 and 3.4 µm thick respectively. Tribological tests were performed by a Pin-on-Disk rotative tribometer with alumina and steel (100Cr6) balls. A comparison of the friction coefficient and the wear rate for each sample has been made. The adhesion of the coatings has been performed by analyzing the wear track using optical profilometry, optical microscopy and scanning electron microscopy equipped with an energy-dispersive X-ray spectrometer. The best tribological performances were observed by combining carbides coatings and carburized 18CrMo4 or reference steel. In contrast, the TiWCN thin film completely delaminated.</dc:description>
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