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Towards in-situ fumes composition monitoring during an additive manufacturing process using energy dispersive X-ray fluorescence spectrometry

Article dans une revue avec comité de lecture
Auteur
ccSTOLIDI, Adrien
ccTOURON, Anthony
ccTOULEMONDE, Loïc
HUGUES PARADIS
ccLAPOUGE, Pierre
86289 Laboratoire Procédés et Ingénierie en Mécanique et Matériaux [PIMM]
ccCOSTE, FREDERIC
86289 Laboratoire Procédés et Ingénierie en Mécanique et Matériaux [PIMM]
JEAN-PAUL GARANDET

URI
http://hdl.handle.net/10985/24798
DOI
10.1016/j.addlet.2023.100153
Date
2023
Journal
Additive Manufacturing Letters

Résumé

We present an in-situ energy dispersive X-ray fluorescence measurement of the content of Chromium and Nickel in the fumes produced by selective laser melting on an Inconel 625 powder. Significant variations of the intensities of the Chromium and Nickel K fluorescence lines were evidenced as a function of the laser power, lasing velocity and chamber atmosphere. Calibration has been carried out using Monte–Carlo particle transport simulations allowed to obtain a quantitative estimate of the Chromium and Nickel mass fraction in the fumes. The experimental data has been compared to the predictions of an analytical physico-chemical model with consistent results. This approach thus also allows to provide information on the temperature of the metallic bath.

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