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Effect of annealing treatment on the microstructure, mechanical and tribological properties of chromium carbonitride coatings

Article dans une revue avec comité de lecture
Author
AISSANI, Linda
421622 Universite Abbes Laghrour [Khenchela]
FELLAH, Mamoun
266547 Université Badji Mokhtar Annaba [UBMA]
421622 Universite Abbes Laghrour [Khenchela]
RADJEHI, Lamia
1685 Laboratoire des Systèmes Mécaniques et d'Ingénierie Simultanée [LASMIS]
421622 Universite Abbes Laghrour [Khenchela]
NOUVEAU, Corinne
127742 Laboratoire Bourguignon des Matériaux et Procédés [LABOMAP]
MONTAGNE, Alex
118112 Institut Pprime [PPRIME]
211915 Mechanics surfaces and materials processing [MSMP]
ALHUSSEIN, Akram
1685 Laboratoire des Systèmes Mécaniques et d'Ingénierie Simultanée [LASMIS]

URI
http://hdl.handle.net/10985/19636
DOI
10.1016/j.surfcoat.2018.12.099
Date
2019
Journal
Surface and Coatings Technology

Abstract

Chromium nitrides were deposited by RF reactive magnetron sputtering from a Cr target on high carbon steel substrates XC100 (1.17 wt% carbon) in a N2 and Ar gas mixture. In order to investigate the formation of chromium nitrides, carbide and carbonitride compounds were subjected to vacuum annealing treatment for 1 h at various temperatures ranging from 700 to 1000 °C. The samples were characterized by EDS, XPS, XRD, SEM, nanoindentation and tribometry. The results showed the emergence of Cr2N and CrN during the early stages of annealing and the appearance of chromium carbonitride phases only at 900 °C. The (111) preferred orientation of the fcc CrN phase was changed to (002) at 900 °C in parallel with the appearance of chromium carbides. Nanoindentation tests revealed a gradual increase of the Young's modulus from 198 to 264 GPa when increasing the annealing temperature, while the hardness showed a maximum value (H = 22.4 GPa) at 900 °C. The low friction coefficient of the Crsingle bondCsingle bondN coating against a 100Cr6 ball was approximately 0.42 at 900 °C. The enhancement of mechanical and tribological properties was attributed to the stronger bonding Crsingle bondC at the CrN/XC100 interfaces as confirmed by XPS results.

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  • Laboratoire Mechanics, Surfaces and Materials Processing (MSMP)

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