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Revisiting Dynamic Fracture in PMMA: The Interplay Between Local and Global Methods

Article dans une revue avec comité de lecture
Auteur
ccFOURNIER, Vincent
1002421 Institut de Mécanique et d'Ingénierie de Bordeaux [I2M]
ccGIRARDOT, Jérémie
1002421 Institut de Mécanique et d'Ingénierie de Bordeaux [I2M]
ccKOPP, Jean-Benoit
1002421 Institut de Mécanique et d'Ingénierie de Bordeaux [I2M]

URI
http://hdl.handle.net/10985/26729
DOI
10.1007/s10704-025-00865-z
Date
2025-06-27
Journal
International Journal of Fracture

Résumé

Polymethyl methacrylate (PMMA) is a benchmark brittle material for dynamic crack propagation studies. Despite extensive research, significant inconsistencies persist in reported fracture parameter values, complicating the establishment of a consensus on their sensitivity to the cracking regime. This study aims to rigorously determine these properties while identifying the origins of these discrepancies. To minimize microbranching effects that can strongly influence fracture surface roughness, crack propagation was restricted to subcritical velocities using a strip-band-specimen (SBS) geometry and a dedicated experimental setup. This approach ensured a quasi-steady propagation regime with minimal inertial effects. Dynamic toughness was evaluated using resistance curves constructed from Williams series expansion and displacement fields obtained via digital image correlation (DIC). Fracture energy was assessed through two complementary methods: a global energy balance and an indirect analytical approach based on Irwin’s generalized relation. Two distinct propagation regimes were identified: a stable regime (90 – 180  $$\hbox {m}.\hbox {s}^{-1}$$ m . s - 1 ) with smooth fracture surfaces and an unstable regime (180 – 320  $$\hbox {m}.\hbox {s}^{-1}$$ m . s - 1 ) characterized by the emergence of conical microstructures, followed by a transition to fully disrupted propagation beyond 320  $$\hbox {m}.\hbox {s}^{-1}$$ m . s - 1 , marking the onset of microbranches. A key outcome of this study is the validation of global fracture energy estimation through the local approach, and vice versa, allowing the derivation of one fracture property from the other – an unprecedented achievement for PMMA in dynamic crack propagation. This was made possible by the experimental setup and specimen geometry, which effectively minimized parasitic effects such as inertia and microbranching. Additionally, the findings confirm a strong correlation between surface roughness and the evolution of fracture energy from the earliest stages of dynamic propagation.

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I2M-IJF-Kopp-2025.pdf
Taille:
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Format:
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Fin d'embargo:
2025-12-09
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  • Institut de Mécanique et d’Ingénierie de Bordeaux (I2M)

Documents liés

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  • Breaking pharmaceutical tablets with a hole: Reevaluation of the stress concentration factor and influence of the hole size 
    Article dans une revue avec comité de lecture
    CROQUELOIS, Benjamin; ccGIRARDOT, Jeremie; ccKOPP, Jean-Benoit; CAZAUTETS, Clément; TCHORELOFF, Pierre; MAZEL, Vincent (Elsevier, 2017)
    Mechanical strength is an important property for pharmaceutical tablets. Its study using the theory of linear elastic fracture mechanics has been introduced in the pharmaceutical field through the Brittle Fracture Index ...
  • Disk-shaped compact tension test for fracture analysis on pharmaceutical tablets 
    Article dans une revue avec comité de lecture
    ccGIRARDOT, Jérémie; ccKOPP, Jean-Benoit; ccCROQUELOIS, Benjamin; ccTCHORELOFF, Pierre; ccMOREL, Stéphane; ccMAZEL, Vincent (Elsevier BV, 2023-01)
    Pharmaceutical tablets must meet a number of requirements and among them, the mechanical strength plays an important role. The diametral compression test is generally used to evaluate it but can generate unstable failures. ...
  • Comparing failure tests on pharmaceutical tablets: Interpretation using experimental results and a numerical approach with cohesive zone models 
    Article dans une revue avec comité de lecture
    ccMAZEL, Vincent; ccGIRARDOT , Jeremie; ccKOPP, Jean-Benoit; MOREL, Stéphane; TCHORELOFF, Pierre (Elsevier BV, 2023-07)
    The mechanical strength is an important quality attribute of pharmaceutical tablets. It can be determined using different failure tests like the Brazilian test or the three-point bending test. Nevertheless, literature shows ...
  • Reevaluation of the diametral compression test for tablets using the flattened disc geometry 
    Article dans une revue avec comité de lecture
    MAZEL, Vincent; ccGUÉRARD, Sandra; CROQUELOIS, Benjamin; ccKOPP, Jean-Benoit; ccGIRARDOT, Jeremie; DIARRA, Harona; BUSIGNIES, Virginie; TCHORELOFF, Pierre (Elsevier, 2016)
    Mechanical strength is an important critical quality attribute for tablets. It is classically measured, in the pharmaceutical field, using the diametral compression test. Nevertheless, due to small contact area between the ...
  • Dynamic Fracture of a Semi-Crystalline Bio-Based Polymer Pipe: Effect of Temperature 
    Article dans une revue avec comité de lecture
    ccKOPP, Jean-Benoit; ccGIRARDOT, Jeremie (Scientific Research Publishing, Inc., 2021)
    The influence of temperature on the resistance to rapid crack propagation of a semi-crystalline bio-based polymer was studied. The experimental results described in this study allow to initiate a first discussion ...

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