Application of multireﬂection grazing incidence method for stress measurements in polished Al–Mg alloy and CrN coating
TypeArticles dans des revues avec comité de lecture
Multi-reﬂection grazing incidence geometry, referred to as MGIXD, characterized by a small and constant incidence angle, was applied to measure low surface stresses in very thin layers of Al–Mg alloy and CrN coating. These two materials were selected in order to deal with the low and high levels of residual stress, respectively. The inﬂuence of different mechanical treatments on residual stresses was studied for Al–Mg samples. It was found that both rolling and mechanical polishing inﬂuence the distribution and amplitude of residual stress in surface layers. In the case of CrN coating, a very high compressive stress was generated during the deposition process. The stress distributions determined by the MGIXD method is in good agreement with the classic sin2 technique results for all studied samples. In performing stress measurements for a powder sample, it was found that the application of the Göbel mirror in the incident beam strongly reduces statistical and misalignment errors. Additionally, the root mean square values of the third order lattice strain within diffracting grains were determined.
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Problem of elastic anisotropy and stacking faults in stress analysis using multireflection grazing-incidence X-ray diffraction MARCISZKO, Marianna; BACZMANSKI, Andrzej; MIROSŁAW, Wrobel; SEILER, Wilfrid; BRAHAM, Chedly; WRONSKI, Sebastian; WAWSZCZAK, Roman (International Union of Crystallography, 2015)Multireflection grazing-incidence X-ray diffraction (MGIXD) was used to determine the stress- and strain-free lattice parameter in the surface layer of mechanically treated (polished and ground) tungsten and austenitic ...
Stress measurements by multi-reflection grazing-incidence X-ray diffraction method (MGIXD) using different radiation wavelengths and different incident angles MARCISZKO, Marianna; BACZMANSKI, Andrzej; BRAHAM, Chedly; WROBEL, Mirosław; WRONSKI, Sebastian; CIOS, Grzegorz (Elsevier, 2017)The presented study introduces the development of the multi-reflection grazing-incidence X-ray diffraction method (MGIXD) for residual stress determination. The proposed new methodology is aimed at obtaining more reliable ...
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MARCISZKO-WIĄCKOWSKA, Marianna; OPONOWICZ, Adrian; BACZMANSKI, Andrzej; WRÓBEL, Mirosław X.; BRAHAM, Chedly; WAWSZCZAK, Roman (International Union of Crystallography, 2019)The multireflection grazing-incidence X-ray diffraction method is used to test surface stresses at depths of several micrometres in the case of metal samples. This work presents new ways of analysing experimental data ...
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